3DXD
Crystal structure of the intracellular domain of human APP (T668E mutant) in complex with Fe65-PTB2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-07-19 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.933 |
Spacegroup name | P 61 |
Unit cell lengths | 115.115, 115.115, 75.254 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.690 - 2.200 |
R-factor | 0.204 |
Rwork | 0.202 |
R-free | 0.24700 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.400 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.062 | 0.432 |
Number of reflections | 28638 | |
<I/σ(I)> | 30.3 | 3.9 |
Completeness [%] | 99.7 | 97.9 |
Redundancy | 10.6 | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.6 | 293 | 3.2 M NaCl, 0.1 M sodium acetate , pH 4.6, VAPOR DIFFUSION, temperature 293K |