9ZYW

[20,21,22] Two turn tensegrity triangle with 20,21, and 22 bp edges

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-11-12
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.000000
Spacegroup name	P 1
Unit cell lengths	65.370, 67.692, 71.762
Unit cell angles	93.94, 104.65, 101.71

Refinement procedure

Resolution	40.710 - 7.110
R-factor	0.1638
Rwork	0.159
R-free	0.25410
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.812
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	68.868	8.435
High resolution limit [Å]	7.105	7.105
Number of reflections	1201	200
<I/σ(I)>	4.5
Completeness [%]	78.9
Redundancy	2.8
CC(1/2)	0.950	0.619

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	293	100 mM MOPS, 1.25 M magnesium sulfate