9YBS

ARID1B ARID bound to compound A-1 (5-(hex-1-yn-1-yl)pyridine-3-carboxylic acid)

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-07-03
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.99987
Spacegroup name	P 65
Unit cell lengths	68.728, 68.728, 45.661
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	36.230 - 1.490
R-factor	0.1712
Rwork	0.170
R-free	0.20230
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.840
Data reduction software	autoPROC
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	59.520	1.550
High resolution limit [Å]	1.490	1.490
Rmerge	0.042	0.212
Rpim	0.015
Number of reflections	16743	455
<I/σ(I)>	23.2	1.6
Completeness [%]	83.2	22.81
Redundancy	7.37	1.44
CC(1/2)	0.999	0.935

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	277	1.5 M sodium citrate, pH 6.5, 0.033% w/v 4-nitrobenzoic acid, 0.033% w/v 5-sulfosalicylic acid dihydrate, 0.033% w/v naphthalene-1,3,6-trisulfonic acid trisodium salt hydrate, 0.002 M HEPES sodium, pH 6.8