9WQ4

Crystal structure of CNOT6L and Cpd1 complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-10-27
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97853
Spacegroup name	P 32 2 1
Unit cell lengths	77.171, 77.171, 169.803
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	26.060 - 2.400
R-factor	0.2086
Rwork	0.206
R-free	0.25430
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.012
RMSD bond angle	1.405
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.440
High resolution limit [Å]	2.400	2.400
Rmerge	0.167	0.010
Number of reflections	23653	1120
<I/σ(I)>	17.66
Completeness [%]	100.0	99.8
Redundancy	14.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	0.1M Hepes, pH 7.5, 1.1M ammonium tartrate, 0.2M NDSB-201