9VZA

Crystal structure of T2R-TTL-TZ5 complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-18
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97853
Spacegroup name	P 21 21 21
Unit cell lengths	104.510, 156.870, 180.740
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	59.240 - 2.610
R-factor	0.2382
Rwork	0.236
R-free	0.27990
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.861
Data reduction software	XDS
Data scaling software	xia2
Phasing software	PHASER
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	60.250	2.660
High resolution limit [Å]	2.610	2.610
Number of reflections	90414	59651
<I/σ(I)>	5.8
Completeness [%]	99.5
Redundancy	12.8
CC(1/2)	0.976	0.333

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7