9VYN

Crystal structure of T2R-TTL-TZ0 complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-18
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97853
Spacegroup name	P 21 21 21
Unit cell lengths	105.280, 157.590, 181.490
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.500 - 2.760
R-factor	0.2334
Rwork	0.232
R-free	0.27140
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.765
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.500	2.830
High resolution limit [Å]	2.760	2.760
Number of reflections	77781	5655
<I/σ(I)>	9.5
Completeness [%]	99.5
Redundancy	13.4
CC(1/2)	0.995	0.578

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7