9VP8

Crystal structure of YdjB from Salmonella enterica subsp. enterica serovar Typhi

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	125
Detector technology	PIXEL
Collection date	2022-09-25
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.000
Spacegroup name	P 43 21 2
Unit cell lengths	42.880, 42.880, 140.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.640 - 1.920
R-factor	0.1917
Rwork	0.191
R-free	0.21150
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.764
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHENIX
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.640	1.989
High resolution limit [Å]	1.920	1.920
Number of reflections	10725	1045
<I/σ(I)>	50.97
Completeness [%]	99.9
Redundancy	25.3
CC(1/2)	1.000	0.999

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293.15	20% w/v PEG 8000 0.1M MES pH 6.0 0.2M Ca(Oac)2