9V0K
UBR box of human UBR1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 5C (4A) |
| Synchrotron site | PAL/PLS |
| Beamline | 5C (4A) |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2024-10-17 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 80.147, 30.165, 63.154 |
| Unit cell angles | 90.00, 113.70, 90.00 |
Refinement procedure
| Resolution | 29.100 - 1.540 |
| R-factor | 0.1745 |
| Rwork | 0.171 |
| R-free | 0.20650 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.059 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 (720) |
| Phasing software | PHENIX (1.20.1-4487) |
| Refinement software | PHENIX (1.20.1-4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.100 | 1.595 |
| High resolution limit [Å] | 1.540 | 1.540 |
| Rmerge | 0.153 | |
| Number of reflections | 38619 | 1958 |
| <I/σ(I)> | 10.92 | |
| Completeness [%] | 97.7 | |
| Redundancy | 6 | |
| CC(1/2) | 0.652 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 295.15 | Sodium phosphate monobasic monohydrate, potassium phosphate dibasic |
