9UOM

Tacheng tick virus 1 nucleoprotein head domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	289
Detector technology	PIXEL
Collection date	2021-04-12
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.97853
Spacegroup name	P 65
Unit cell lengths	114.260, 114.260, 54.863
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	37.400 - 1.590
R-factor	0.1602
Rwork	0.159
R-free	0.18310
Structure solution method	MAD
RMSD bond length	0.008
RMSD bond angle	0.952
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	AutoSol
Refinement software	PHENIX (v1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.650
High resolution limit [Å]	1.590	1.590
Number of reflections	55047	55047
<I/σ(I)>	11.8
Completeness [%]	99.7
Redundancy	19.7
CC(1/2)	0.969	0.969

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	LIQUID DIFFUSION		289.15	0.2M LiSO4,20%PEG 3350