9TBL
SSX Lysozyme at 100K
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX IV BEAMLINE BioMAX |
| Synchrotron site | MAX IV |
| Beamline | BioMAX |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2025-11-18 |
| Detector | DECTRIS EIGER2 X CdTe 16M |
| Wavelength(s) | 0.7293 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 77.160, 77.160, 37.500 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 22.060 - 1.750 |
| Rwork | 0.165 |
| R-free | 0.21130 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.973 |
| Data reduction software | CrystFEL |
| Data scaling software | CrystFEL |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0431 (refmacat 0.4.105)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 22.060 | 1.930 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Number of reflections | 11932 | 575 |
| <I/σ(I)> | 19.88 | |
| Completeness [%] | 100.0 | |
| Redundancy | 339 | |
| CC(1/2) | 0.997 | 0.836 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 293 | 19.04% NaCl, 5.44% PEG 8,000, 68mM Na Acetate pH 3.0 |
