9T6J

Complement C5 re-refined

Replaces:  3CU7

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MAX II BEAMLINE I711
Synchrotron site	MAX II
Beamline	I711
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	1998-10-20
Detector	MAR scanner 345 mm plate
Wavelength(s)	0.989
Spacegroup name	P 31
Unit cell lengths	144.260, 144.260, 241.000
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	29.290 - 3.110
R-factor	0.236
Rwork	0.234
R-free	0.26860
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.749
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	3.210
High resolution limit [Å]	3.100	3.100
Rmerge	0.040	0.570
Number of reflections	98600	8671
<I/σ(I)>	13.5	1.3
Completeness [%]	96.9
Redundancy	1.36

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	6.8	277	100 mM NaCl, MES pH 6.8