9SZY

PCSK9 CTD fragment structure

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MAX IV BEAMLINE BioMAX
Synchrotron site	MAX IV
Beamline	BioMAX
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-04-21
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.976254
Spacegroup name	P 21 21 21
Unit cell lengths	62.602, 70.121, 148.039
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	74.020 - 1.759
R-factor	0.2003
Rwork	0.198
R-free	0.23620
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.980
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	BUSTER (2.11.8)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	74.020	1.984
High resolution limit [Å]	1.759	1.759
Number of reflections	39086	1955
<I/σ(I)>	10.5
Completeness [%]	59.7
Redundancy	6.6
CC(1/2)	0.998	0.538

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	25 mM HEPES pH 7.5 300 mM NaCl 5% glycerol