Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-08-08 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.95373 |
| Spacegroup name | P 6 2 2 |
| Unit cell lengths | 149.345, 149.345, 53.965 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.340 - 1.768 |
| R-factor | 0.2366 |
| Rwork | 0.235 |
| R-free | 0.25840 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.870 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.8) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 129.337 | 1.988 |
| High resolution limit [Å] | 1.768 | 1.768 |
| Number of reflections | 22512 | 1126 |
| <I/σ(I)> | 18.5 | |
| Completeness [%] | 95.7 | |
| Redundancy | 19.7 | |
| CC(1/2) | 0.999 | 0.837 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.6 ammonium sulfate, 10 % dioxane, 0.1 M Mes pH 6.5 |
