9RTJ
Hydrid structure of the helix bundle domain of pRN1 primase in complex with DNA, ATP and dGTP
Spectrometer
Experimental method: SOLID-STATE NMR, SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE III HD | 900 | |
| 2 | Bruker | AVANCE NEO | 700 | |
| 3 | Bruker | AVANCE NEO | 600 | |
| 4 | Bruker | AVANCE III | 500 | |
| 5 | Bruker | AVANCE III | 850 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D HNCA |
| 10 | 2 | 4 | 3D 1H-13C NOESY aliphatic |
| 11 | 1 | 3 | 3D 1H-13C NOESY aliphatic |
| 12 | 1 | 3 | 3D 1H-13C NOESY aromatic |
| 13 | 2 | 4 | 3D 1H-13C NOESY aromatic |
| 14 | 1 | 3 | 2D 1H-13C HSQC aromatic |
| 15 | 1 | 3 | 2D 1H-13C HSQC aliphatic |
| 16 | 2 | 2 | 2D-F1fF2f-NOESY |
| 17 | 2 | 2 | 2D-F2f-NOESY |
| 18 | 1 | 3 | 3D-13C-aliphatic-HfilteredHedited-NOESY |
| 19 | 1 | 3 | 3D-13C-aromatic-HfilteredHedited-NOESY |
| 2 | 1 | 1 | 3D HN(CA)CO |
| 20 | 2 | 5 | 2D-imino-NOESY |
| 21 | 4 | 8 | 2D-natural-abundance-Nhsqc |
| 22 | 2 | 6 | 2D-natural-abundance-Chsqc-aliphatic |
| 23 | 2 | 6 | 2D-natural-abundance-Chsqc-aromatic |
| 24 | 1 | 1 | 2D 1H-15N HSQC |
| 25 | 1 | 3 | 2D 1H-15N HSQC |
| 26 | 5 | 9 | CHHP |
| 27 | 5 | 9 | NHHP |
| 28 | 5 | 7 | hPH |
| 29 | 5 | 10 | hPH |
| 3 | 1 | 1 | 3D HN(CO)CA |
| 4 | 1 | 1 | 3D HNCACB |
| 5 | 1 | 1 | 3D CBCA(CO)NH |
| 6 | 1 | 1 | 3D HNCO |
| 7 | 1 | 1 | 3D C(CO)NH |
| 8 | 1 | 1 | 3D H(CCO)NH |
| 9 | 1 | 1 | 3D 1H-15N NOESY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 7 | 1 | 298 |
| 2 | 7 | 1 | 298 |
| 3 | 7 | 1 | 298 |
| 4 | 7 | 1 | 298 |
| 5 | 7 | 1 | 278 |
Conformers
| Conformers Calculated Total Number | 500 |
| Conformers Submitted Total Number | 20 |
