Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-06-04 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.870, 100.430, 104.530 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 72.421 - 1.897 |
Rwork | 0.205 |
R-free | 0.25240 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.544 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0405) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.421 | 2.123 |
High resolution limit [Å] | 1.897 | 1.897 |
Rmerge | 0.125 | 1.151 |
Rpim | 0.036 | 0.448 |
Number of reflections | 37327 | 1867 |
<I/σ(I)> | 13.9 | 1.8 |
Completeness [%] | 93.3 | |
Redundancy | 12.5 | |
CC(1/2) | 1.000 | 0.619 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 30mM sodium nitrate, 30mM disodium hydrogen phosphate, 30mM ammonium sulfate, 100mM MES-imidazole pH 6.5, 20%(w/v) PEG 550 MME, 10%(w/v) PEG 20K (Morpheus condition C1) |