9RDQ

SUDV VP40 in complex with LL060

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-04-10
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1.000009
Spacegroup name	C 1 2 1
Unit cell lengths	62.794, 91.169, 48.313
Unit cell angles	90.00, 94.64, 90.00

Refinement procedure

Resolution	45.580 - 1.960
R-factor	0.1858
Rwork	0.185
R-free	0.20490
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.868
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.580	2.030
High resolution limit [Å]	1.960	1.960
Number of reflections	19297	1893
<I/σ(I)>	15.32	5.61
Completeness [%]	98.9	98.13
Redundancy	6.9	6.9
CC(1/2)	0.998	0.967

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	100 mM HEPES, 40 mM MgCl2, 10% (v/v) PEG400, 20% ethylen glycol as cryoprotectant