9RB2
Crystal Structure of glxR
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-07-08 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.9537 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 79.176, 109.209, 146.695 |
| Unit cell angles | 90.00, 93.39, 90.00 |
Refinement procedure
| Resolution | 73.220 - 2.210 |
| R-factor | 0.236 |
| Rwork | 0.235 |
| R-free | 0.27320 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.980 |
| Data reduction software | XDS |
| Data scaling software | DIALS |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.4 (10-JUL-2024)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 73.220 | 2.250 |
| High resolution limit [Å] | 2.210 | 2.210 |
| Rmerge | 0.446 | 2.809 |
| Rmeas | 0.481 | 3.020 |
| Rpim | 0.178 | 1.104 |
| Total number of observations | 441421 | 22669 |
| Number of reflections | 61556 | 3061 |
| <I/σ(I)> | 4.6 | 0.7 |
| Completeness [%] | 98.7 | |
| Redundancy | 7.2 | 7.4 |
| CC(1/2) | 0.978 | 0.351 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 293 | 25 %v/v PEGSM, 0.1 M Na Acet 4.5 pH |
