9RAP

VDR complex with UG-635

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 2
Synchrotron site	SOLEIL
Beamline	PROXIMA 2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2025-03-27
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.98
Spacegroup name	P 65 2 2
Unit cell lengths	65.860, 65.860, 263.080
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	47.810 - 2.200
R-factor	0.202
Rwork	0.197
R-free	0.24860
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.883
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.810	2.280
High resolution limit [Å]	2.200	2.200
Number of reflections	18114	1746
<I/σ(I)>	21.35
Completeness [%]	99.6
Redundancy	2
CC(1/2)	0.999	0.967

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	290	3M Na Acetate 0.1M Tris HCl pH8