Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE MASSIF-1 |
| Synchrotron site | ESRF |
| Beamline | MASSIF-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-11-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9897 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 75.694, 64.748, 76.394 |
| Unit cell angles | 90.00, 92.02, 90.00 |
Refinement procedure
| Resolution | 75.650 - 2.300 |
| R-factor | 0.198 |
| Rwork | 0.195 |
| R-free | 0.25190 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.886 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.650 | 2.380 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Number of reflections | 60362 | 3299 |
| <I/σ(I)> | 23.91 | |
| Completeness [%] | 99.3 | |
| Redundancy | 3.1 | |
| CC(1/2) | 0.968 | 0.968 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | 12% PEG3350, 50-90 mM Ammonium citrate |
