Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE MASSIF-1 |
| Synchrotron site | ESRF |
| Beamline | MASSIF-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-12-02 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9897 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 83.503, 109.666, 124.417 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 35.180 - 1.970 |
| R-factor | 0.2149 |
| Rwork | 0.213 |
| R-free | 0.25280 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.963 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.180 | 2.040 |
| High resolution limit [Å] | 1.970 | 1.970 |
| Number of reflections | 72605 | 3960 |
| <I/σ(I)> | 7.39 | |
| Completeness [%] | 97.4 | |
| Redundancy | 1.9 | |
| CC(1/2) | 0.993 | 0.444 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | 12% PEG3350, 50-90 mM Ammonium citrate |
