9QK4

X-ray crystal structure of SlPYL1-Ferulic Acid complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-14
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.979
Spacegroup name	P 32 2 1
Unit cell lengths	89.642, 89.642, 50.369
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.820 - 2.000
R-factor	0.2298
Rwork	0.228
R-free	0.26590
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.499
Data reduction software	autoPROC
Data scaling software	autoPROC
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.930	2.072
High resolution limit [Å]	2.000	2.000
Number of reflections	14889	761
<I/σ(I)>	2.86
Completeness [%]	92.6
Redundancy	1.35
CC(1/2)	0.870	0.870

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	MICROBATCH	7	295	3.5 M ammonium sulfate pH 7.0