9Q8U
Complex of Caprine Serum Albumin with Cefaclor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-04-16 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.918409 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 42.846, 67.580, 214.807 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 42.040 - 1.760 |
| R-factor | 0.18163 |
| Rwork | 0.180 |
| R-free | 0.22758 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.019 |
| RMSD bond angle | 2.014 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.040 | 1.880 |
| High resolution limit [Å] | 1.700 | 1.770 |
| Rmerge | 0.041 | 0.589 |
| Rmeas | 0.049 | 0.707 |
| Number of reflections | 60997 | 9378 |
| <I/σ(I)> | 18.61 | 1.85 |
| Completeness [%] | 98.0 | 94.7 |
| Redundancy | 3.2 | 2.8 |
| CC(1/2) | 0.999 | 0.635 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | Jeffamine ED-2001, Ba2+, Na2+, Cl-, Citrate buffer |
