9PHP

[19-7B AG] 19 bp tensegrity triangle that propagates via blunt-end stacking with A stacking on G at the interface

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-12-11
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.007430
Spacegroup name	I 41 3 2
Unit cell lengths	157.020, 157.020, 157.020
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.480 - 4.330
R-factor	0.1794
Rwork	0.178
R-free	0.20410
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.659
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	64.103	64.103	4.591
High resolution limit [Å]	4.328	10.445	4.328
Number of reflections	2217	200	201
<I/σ(I)>	31.4
Completeness [%]	92.3
Redundancy	67.5
CC(1/2)	1.000	1.000	0.772

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	100 mM MOPS, 1.25 M magnesium sulfate