9OK4

GID4 in complex with CLEO4-88 and ACAA1

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-01-24
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.952993
Spacegroup name	P 21 21 21
Unit cell lengths	60.941, 92.993, 202.583
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.430 - 2.280
R-factor	0.1916
Rwork	0.190
R-free	0.22950
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.562
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.430	2.362
High resolution limit [Å]	2.280	2.280
Number of reflections	53445	5268
<I/σ(I)>	10.76
Completeness [%]	99.7	98.92
Redundancy	9.98
CC(1/2)	0.997	0.537

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	20% PEG3350, 0.1 M Tris pH 7.5 and 0.2 M NaF