Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2022-10-25 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.95373 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 88.804, 88.804, 157.198 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 44.400 - 2.900 |
| Rwork | 0.234 |
| R-free | 0.27170 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.21rc1_5107: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.400 | 3.080 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rmerge | 0.125 | 1.741 |
| Rmeas | 0.132 | |
| Rpim | 0.042 | 0.567 |
| Total number of observations | 165992 | |
| Number of reflections | 16511 | 2621 |
| <I/σ(I)> | 13.8 | |
| Completeness [%] | 100.0 | |
| Redundancy | 10.1 | 10.3 |
| CC(1/2) | 0.993 | 0.653 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 9.46 | 293 | 0.1 M CHES pH 9.46 1.05 M tri-Na Citrate 0.025 M tri-glycine |
