Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-03-21 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.95373 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 90.350, 87.610, 89.500 |
| Unit cell angles | 90.00, 113.98, 90.00 |
Refinement procedure
| Resolution | 43.840 - 2.420 |
| R-factor | 0.18506 |
| Rwork | 0.183 |
| R-free | 0.22761 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.718 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | FFT |
| Refinement software | REFMAC (5.8.0430) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.840 | 2.500 |
| High resolution limit [Å] | 2.420 | 2.420 |
| Number of reflections | 20893 | 7228 |
| <I/σ(I)> | 16.2 | |
| Completeness [%] | 89.9 | |
| Redundancy | 6.9 | |
| CC(1/2) | 0.999 | 0.681 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 277 | 0.2M tri-Sodium citrate 18 % w/v PEG 3,350 |
