Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-07-03 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 114.372, 54.056, 44.603 |
| Unit cell angles | 90.00, 101.04, 90.00 |
Refinement procedure
| Resolution | 48.700 - 1.871 |
| R-factor | 0.2086 |
| Rwork | 0.207 |
| R-free | 0.23120 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.000 |
| Data reduction software | autoPROC |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.8) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.700 | 1.970 |
| High resolution limit [Å] | 1.870 | 1.870 |
| Number of reflections | 20120 | 2136 |
| <I/σ(I)> | 7.9 | |
| Completeness [%] | 90.5 | |
| Redundancy | 3.2 | |
| CC(1/2) | 0.996 | 0.477 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | 25% Peg 1500, 0.1M MIB pH 7.0 |
