9NUB

NMR solution structure of unmodified human matrix Gla protein

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III		600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	2	2D 1H-15N HSQC
10	1	2	3D 1H-15N TOCSY
11	1	2	3D 1H-15N NOESY
12	1	2	3D 1H-13C NOESY aliphatic
13	1	2	3D 1H-13C NOESY aromatic
14	1	2	T1/R1 relaxation
15	1	2	T2/R2 relaxation
16	1	2	1H-15N heteronoe
2	1	1	3D HNCO
3	1	1	3D HN(CA)CO
4	1	1	3D CBCANH
5	1	1	3D (H)CC(CO)NH
6	1	2	3D HCCH-TOCSY
7	1	1	3D (H)N(CA)NNH
8	1	1	3D (H)N(COCA)NNH

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	5.7	1	280

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20