9NDB

[4,7,8-2] Shifted tensegrity triangle with an (arm,center,arm) distribution of (4,7,8) base pairs and 2 nt sticky ends

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-10-16
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.000010
Spacegroup name	H 3
Unit cell lengths	108.119, 108.119, 90.550
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	32.960 - 4.070
R-factor	0.163
Rwork	0.162
R-free	0.17280
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.733
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	65.091	65.091	4.518
High resolution limit [Å]	4.070	10.261	4.074
Number of reflections	2180	198	197
<I/σ(I)>	14.5
Completeness [%]	86.7
Redundancy	10.7
CC(1/2)	1.000	1.000	0.348

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	100 mM MOPS, 1.25 M magnesium sulfate