Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL9-2 |
| Synchrotron site | SSRL |
| Beamline | BL9-2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-11-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97946 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 42.994, 183.065, 50.451 |
| Unit cell angles | 90.00, 98.48, 90.00 |
Refinement procedure
| Resolution | 38.630 - 1.600 |
| R-factor | 0.1837 |
| Rwork | 0.182 |
| R-free | 0.20690 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.982 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.21.2_5419) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.630 | 1.630 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmeas | 0.080 | |
| Rpim | 0.039 | 0.577 |
| Number of reflections | 99666 | 4852 |
| <I/σ(I)> | 9.8 | 1.3 |
| Completeness [%] | 98.6 | |
| Redundancy | 4 | |
| CC(1/2) | 0.997 | 0.491 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M lithium chloride, 20% PEG 3350 |
