9MS4
Crystal structure of an expansin (Xa_EXLX1) from Xanthomonas sacchari
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL12-2 |
| Synchrotron site | SSRL |
| Beamline | BL12-2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-09-01 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.97946 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 201.205, 47.884, 201.435 |
| Unit cell angles | 90.00, 90.17, 90.00 |
Refinement procedure
| Resolution | 90.110 - 2.300 |
| R-factor | 0.1908 |
| Rwork | 0.188 |
| R-free | 0.23980 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.932 |
| Data reduction software | autoPROC |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((1.21.2_5419: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 90.110 | 2.340 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmeas | 0.178 | |
| Rpim | 0.092 | 0.783 |
| Number of reflections | 85530 | 4196 |
| <I/σ(I)> | 7.2 | |
| Completeness [%] | 99.0 | |
| Redundancy | 7 | |
| CC(1/2) | 0.994 | 0.572 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.05 M Hepes pH 6.8, PEG 4000, silver bullet #1 |
