9MFI

Cu-MAHF-9 A8S Metal Alpha-Helix Framework

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MAX IV BEAMLINE BioMAX
Synchrotron site	MAX IV
Beamline	BioMAX
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-10-20
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.688797
Spacegroup name	P 1
Unit cell lengths	10.395, 16.286, 20.196
Unit cell angles	80.28, 87.88, 71.66

Refinement procedure

Resolution	9.950 - 0.890
R-factor	0.081
Rwork	0.081
R-free	0.08130
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	1.926
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	15.250	0.900
High resolution limit [Å]	0.890	0.890
Number of reflections	21942	12
<I/σ(I)>	7.12
Completeness [%]	86.4
Redundancy	2
CC(1/2)	0.994	0.533

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SLOW COOLING		298	water, acetonitrile, copper acetate, methanol