9M6M
Atomic-Level Architecture and Assembly Mechanism of High-order Structures of RIPK1 Fibril Network Revealed by Integrated Structural Biology
Spectrometer
Experimental method: SOLID-STATE NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | 3.2 mm HCN E-free probe | 700 | |
| 2 | Bruker | 0.7 mm HCN probe | 700 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 2 | 1 | 2D DARR 50ms |
| 10 | 1 | 1 | 2D NCACX |
| 11 | 1 | 2 | 2D [2]-13C-DARR 50ms |
| 13 | 1 | 2 | 2D [2]-13C-DARR 500ms |
| 14 | 2 | 1 | 2D DARR 500ms |
| 15 | 2 | 1 | 2D DARR 200ms |
| 16 | 1 | 4 | 2D TEDOR |
| 17 | 1 | 2 | 2D TEDOR |
| 18 | 1 | 2 | 2D [2]-13C-DARR 200ms |
| 2 | 1 | 1 | 3D CaNH |
| 3 | 1 | 1 | 3D coCAcoNH |
| 4 | 3 | 3 | 2D CH |
| 6 | 1 | 1 | 3D hCANCOCX |
| 8 | 1 | 1 | 3D hNCaCx |
| 9 | 1 | 1 | 2D NCOCX |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 5 | 1 | 263 |
| 2 | 5 | 1 | 293 |
| 3 | 5 | 1 | 279 |
Conformers
| Conformers Calculated Total Number | 192 |
| Conformers Submitted Total Number | 10 |
