9M1A
Vitamin D receptor complex with a diethyldiphenylsilane derivative
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-03-12 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.98 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 154.307, 41.785, 42.274 |
| Unit cell angles | 90.00, 96.28, 90.00 |
Refinement procedure
| Resolution | 40.320 - 1.780 |
| R-factor | 0.1808 |
| Rwork | 0.179 |
| R-free | 0.21120 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2zlc |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.783 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.020 | 1.820 |
| High resolution limit [Å] | 1.780 | 1.780 |
| Rmerge | 0.047 | 0.665 |
| Number of reflections | 25689 | 1464 |
| <I/σ(I)> | 14.6 | 2 |
| Completeness [%] | 99.1 | 99.8 |
| Redundancy | 3.3 | |
| CC(1/2) | 0.999 | 0.998 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG 3350, Tacsimate, pH 7.0 |
