Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 98.15 |
| Detector technology | PIXEL |
| Collection date | 2021-11-03 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.95365 |
| Spacegroup name | P 41 3 2 |
| Unit cell lengths | 210.242, 210.242, 210.242 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.279 - 2.300 |
| Rwork | 0.191 |
| R-free | 0.20930 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.447 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.300 | 2.350 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 1.200 | |
| Number of reflections | 70655 | 4480 |
| <I/σ(I)> | 17.5 | |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 3.6 | |
| CC(1/2) | 0.999 | 0.429 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293.15 | Tris pH 7.5, (NH4)2SO4 |
