Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL10U2 |
| Synchrotron site | SSRF |
| Beamline | BL10U2 |
| Temperature [K] | 153 |
| Detector technology | PIXEL |
| Collection date | 2024-04-20 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.97918 |
| Spacegroup name | P 41 |
| Unit cell lengths | 124.588, 124.588, 138.564 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 88.100 - 1.940 |
| R-factor | 0.1869 |
| Rwork | 0.185 |
| R-free | 0.21850 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.793 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.21.1_5286: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 88.100 | 1.990 |
| High resolution limit [Å] | 1.940 | 1.940 |
| Number of reflections | 155895 | 11501 |
| <I/σ(I)> | 8 | |
| Completeness [%] | 100.0 | |
| Redundancy | 12.7 | |
| CC(1/2) | 0.998 | 0.673 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277 | 0.1 M HEPES pH 7.5, 30% w/v Polyethylene glycol 1,000 |
