9LQC
Crystal structure of NrN D119A in complex with SAH-AMP
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL10U2 |
| Synchrotron site | SSRF |
| Beamline | BL10U2 |
| Temperature [K] | 153 |
| Detector technology | PIXEL |
| Collection date | 2024-04-20 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.97918 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 66.668, 121.609, 72.579 |
| Unit cell angles | 90.00, 90.31, 90.00 |
Refinement procedure
| Resolution | 72.580 - 2.370 |
| R-factor | 0.2569 |
| Rwork | 0.255 |
| R-free | 0.29290 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.752 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.21.1_5286: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 72.730 | 2.440 |
| High resolution limit [Å] | 2.370 | 2.380 |
| Number of reflections | 46516 | 3422 |
| <I/σ(I)> | 4 | |
| Completeness [%] | 100.0 | |
| Redundancy | 6.5 | |
| CC(1/2) | 0.830 | 0.235 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 0.1 M Succinic acid pH 7.0, 15% w/v Polyethylene glycol 3,350 |
