Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NFPSS BEAMLINE BL19U1 |
| Synchrotron site | NFPSS |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-12-10 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97861 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 105.087, 156.675, 183.659 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 91.210 - 2.590 |
| R-factor | 0.2292 |
| Rwork | 0.226 |
| R-free | 0.29610 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond angle | 17.266 |
| Data reduction software | xia2 |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 91.830 | 2.630 |
| High resolution limit [Å] | 2.590 | 2.590 |
| Number of reflections | 94149 | 4673 |
| <I/σ(I)> | 7.3 | |
| Completeness [%] | 99.2 | |
| Redundancy | 13.3 | |
| CC(1/2) | 0.993 | 0.486 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7 |
