9LM7
Crystal structrue of bvFP-Pr1-88.4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | Cu FINE FOCUS |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-07-08 |
| Detector | RIGAKU HyPix-6000HE |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 153.921, 81.656, 84.443 |
| Unit cell angles | 90.00, 95.72, 90.00 |
Refinement procedure
| Resolution | 29.280 - 1.800 |
| R-factor | 0.1981 |
| Rwork | 0.198 |
| R-free | 0.22120 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.010 |
| Data reduction software | CrysalisPro |
| Data scaling software | CrysalisPro |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.280 | 1.864 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 96135 | 9419 |
| <I/σ(I)> | 37.08 | |
| Completeness [%] | 99.6 | |
| Redundancy | 3.2 | |
| CC(1/2) | 1.000 | 0.966 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 300 | 1.1 M ammonium tartrate dibasic (pH 7.0), 10% v/v 2-propanol |
