Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2023-09-05 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.987 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 76.984, 83.841, 59.184 |
| Unit cell angles | 90.00, 101.91, 90.00 |
Refinement procedure
| Resolution | 28.960 - 1.495 |
| R-factor | 0.1668 |
| Rwork | 0.166 |
| R-free | 0.18470 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.854 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.960 | 1.550 |
| High resolution limit [Å] | 1.459 | 1.500 |
| Number of reflections | 58485 | 5563 |
| <I/σ(I)> | 2 | |
| Completeness [%] | 98.5 | |
| Redundancy | 5 | |
| CC(1/2) | 0.987 | 0.884 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | 0.2M MgCl2, 0.1M sodium citrate (pH 5.0), 10% PEG 20000 |
