9LFQ
Complex crystal structure of transaldolase AprG with GlcNAc from Streptoalloteichus tenebrarius
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | LIQUID ANODE |
| Source details | BRUKER METALJET |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-01-17 |
| Detector | Bruker PHOTON III |
| Wavelength(s) | 1.34138 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 52.888, 140.715, 130.775 |
| Unit cell angles | 90.00, 101.49, 90.00 |
Refinement procedure
| Resolution | 36.870 - 2.130 |
| R-factor | 0.2298 |
| Rwork | 0.228 |
| R-free | 0.26260 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.463 |
| Data reduction software | SAINT |
| Data scaling software | SAINT |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.21.1_5286: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.420 | 2.160 |
| High resolution limit [Å] | 2.130 | 2.130 |
| Rmerge | 0.119 | 0.448 |
| Number of reflections | 104303 | 4239 |
| <I/σ(I)> | 7.66 | |
| Completeness [%] | 99.8 | |
| Redundancy | 5.23 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 0.15 M Sodium acetate trihydrate; 29% polyethylene glycol 4,000; 0.1 M Tris ;pH 8.5 |
