Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NFPSS BEAMLINE BL19U1 |
| Synchrotron site | NFPSS |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-06-02 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9793 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 68.980, 68.980, 78.920 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 34.490 - 1.570 |
| R-factor | 0.2136 |
| Rwork | 0.212 |
| R-free | 0.23530 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.021 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.19_4092: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.460 | 1.610 |
| High resolution limit [Å] | 1.570 | 1.570 |
| Rmerge | 0.118 | 2.109 |
| Rmeas | 0.122 | 2.166 |
| Rpim | 0.028 | 0.489 |
| Total number of observations | 565225 | 43954 |
| Number of reflections | 30688 | 2265 |
| <I/σ(I)> | 20.2 | 1.7 |
| Completeness [%] | 99.4 | |
| Redundancy | 18.4 | 19.4 |
| CC(1/2) | 1.000 | 0.851 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 277 | 2.6M AMMONIUM SULPHATE, 0.1M HEPES BUFFER PH7.5, 1% PEG 400 |
