9KUP
Crystal structure of MCP2201LBD
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 295 |
| Detector technology | PIXEL |
| Collection date | 2013-05-25 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.987 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 59.800, 59.800, 158.201 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 43.328 - 1.500 |
| R-factor | 0.1647 |
| Rwork | 0.164 |
| R-free | 0.18480 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.282 |
| Data scaling software | XDS |
| Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 43.370 | 1.420 |
| High resolution limit [Å] | 1.400 | 1.400 |
| Rmerge | 0.578 | 0.813 |
| Number of reflections | 55393 | 734 |
| <I/σ(I)> | 18.3 | |
| Completeness [%] | 84.6 | 23.5 |
| Redundancy | 16.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 295.15 | 1.8 M Ammonium sulfate, 5% Glycerol |
