9KT2

The crystal structure of BD1 in complex with BDS4

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CAMD BEAMLINE GCPCC
Synchrotron site	CAMD
Beamline	GCPCC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-11-25
Detector	DECTRIS PILATUS 300K
Wavelength(s)	0.978
Spacegroup name	P 21 21 21
Unit cell lengths	35.114, 55.444, 57.530
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.972 - 1.462
R-factor	0.169022743704
Rwork	0.166
R-free	0.19472
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.392
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	PHENIX (1.9_1692+SVN)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.980	1.513
High resolution limit [Å]	1.461	1.461
Number of reflections	20044	20044
<I/σ(I)>	15
Completeness [%]	99.7
Redundancy	9.8
CC(1/2)	0.998	0.998

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289.15	0.15 M potassium bromide, 30% (v/v) PEG2000MME