Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL02U1 |
| Synchrotron site | SSRF |
| Beamline | BL02U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-09-15 |
| Detector | DECTRIS EIGER2 S 9M |
| Wavelength(s) | 0.97895 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 80.557, 119.461, 47.406 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.700 - 1.770 |
| R-factor | 0.1901 |
| Rwork | 0.188 |
| R-free | 0.23480 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.985 |
| Data reduction software | DIALS |
| Data scaling software | DIALS |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 118.710 | 1.700 |
| High resolution limit [Å] | 1.660 | 1.660 |
| Number of reflections | 54000 | 3930 |
| <I/σ(I)> | 7 | |
| Completeness [%] | 100.0 | 99.9 |
| Redundancy | 12.2 | 12.3 |
| CC(1/2) | 0.974 | 0.247 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 289.15 | 20% w/v polyethylene glycol 3350, 0.2 M Calcium acetate hydrate |
