9KOP
Crystal structure of the Trove domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-10-18 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97853 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 63.877, 60.124, 65.590 |
| Unit cell angles | 90.00, 100.61, 90.00 |
Refinement procedure
| Resolution | 49.790 - 1.990 |
| R-factor | 0.1753 |
| Rwork | 0.174 |
| R-free | 0.19990 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.079 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX (1.20.1) |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 64.470 | 2.100 |
| High resolution limit [Å] | 1.990 | 1.990 |
| Rmerge | 0.067 | 0.490 |
| Number of reflections | 33397 | 4818 |
| <I/σ(I)> | 14 | 2.6 |
| Completeness [%] | 99.8 | |
| Redundancy | 3.9 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 290 | 25% PEG 4000, 0.1 M MES,pH 6.0, 6% Tacsimate,pH 6.0 |
