Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL10U2 |
| Synchrotron site | SSRF |
| Beamline | BL10U2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-03-17 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.97918 |
| Spacegroup name | P 32 |
| Unit cell lengths | 55.731, 55.731, 40.448 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 24.130 - 1.840 |
| R-factor | 0.2356 |
| Rwork | 0.234 |
| R-free | 0.27520 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.562 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 24.130 | 1.909 |
| High resolution limit [Å] | 1.840 | 1.844 |
| Number of reflections | 11388 | 6484 |
| <I/σ(I)> | 17.81 | |
| Completeness [%] | 92.4 | |
| Redundancy | 9.1 | |
| CC(1/2) | 0.999 | 0.428 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 292 | 0.2 M sodium formate and 20% (m/v) PEG3350 |
