Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-03-24 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.464, 77.520, 111.475 |
| Unit cell angles | 90.00, 92.19, 90.00 |
Refinement procedure
| Resolution | 40.430 - 1.770 |
| R-factor | 0.17083 |
| Rwork | 0.169 |
| R-free | 0.20294 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.694 |
| Data reduction software | xia2 |
| Refinement software | REFMAC (5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.430 | 1.800 |
| High resolution limit [Å] | 1.770 | 1.770 |
| Number of reflections | 85099 | 4134 |
| <I/σ(I)> | 9.5 | |
| Completeness [%] | 99.7 | |
| Redundancy | 3.3 | |
| CC(1/2) | 0.997 | 0.526 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Tris-HCl pH 8.0, 20%(w/v) PEG6000, and 0.2 M CaCl2 |
