Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-10-09 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.608, 77.679, 111.062 |
| Unit cell angles | 90.00, 92.75, 90.00 |
Refinement procedure
| Resolution | 55.470 - 1.530 |
| R-factor | 0.18391 |
| Rwork | 0.183 |
| R-free | 0.20399 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.742 |
| Data reduction software | xia2 |
| Phasing software | REFMAC (5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.470 | 1.560 |
| High resolution limit [Å] | 1.530 | 1.530 |
| Number of reflections | 131645 | 6510 |
| <I/σ(I)> | 8.2 | |
| Completeness [%] | 99.7 | |
| Redundancy | 3.2 | |
| CC(1/2) | 0.996 | 0.604 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Tris-HCl pH 8.0, 20%(w/v) PEG6000, and 0.2 M CaCl2 |
