9JZ7

PfDXR - Mn2+ - MAMK150 ternary complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-12-09
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.9
Spacegroup name	P 1 21 1
Unit cell lengths	51.749, 77.580, 111.575
Unit cell angles	90.00, 92.60, 90.00

Refinement procedure

Resolution	39.670 - 1.790
R-factor	0.16379
Rwork	0.162
R-free	0.19373
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.009
RMSD bond angle	1.751
Data reduction software	xia2
Refinement software	REFMAC (5)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.650	1.820
High resolution limit [Å]	1.790	1.790
Number of reflections	82163	3917
<I/σ(I)>	8.4
Completeness [%]	98.6
Redundancy	2.7
CC(1/2)	0.992	0.525

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1 M Tris-HCl pH 8.0, 20%(w/v) PEG6000, and 0.2 M CaCl2